An Introduction to the Chemistry of Complex Compounds by Aleksander Abramovich Grinberg

By Aleksander Abramovich Grinberg

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F o u r molecules of water can be removed from t h e compound [Co(NH 3 ) 5 H 2 0] 2 (C 2 0 4 ) 3 • 4 H 2 0 without causing co-ordination of t h e anion, a n d only t h e removal of t h e fifth a n d sixth molecules of water brings a b o u t a transition of t h e oxalate ions t o a nonionic state. This indicates t h a t four molecules of water in t h e compound [Co(NH 3 ) 5 H 2 0] 2 (C 2 0 4 ) 3 • 4 H 2 0 are n o t co-ordinated b u t are b o u n d in a n o t h e r way, perhaps b y the a t t r a c t i o n of t h e electrostatic fields of t h e complex cation a n d anions.

As for the chlorine, it is not co-ordinated as shown by the instantaneous precipitation of silver chloride in the cold. These results lead to the conclusion that the salt has the structure [Co(NH3)4C03]Cl. This structure is supported by the measurement of the molar conductance which yields a value characteristic of a binary electrolyte. V (J, V fJL 128 256 90 92 512 1024 94 96 Thus, the C0 3 -group is co-ordinated in this compound. However, it is known that different anions differ from one another greatly in the tenacity with which they are bound.

For t h e croceo-flaveo n i t r a t e t h e values are V fJL 250 500 1000 95 97 98 I n connection with t h e question of t h e n a t u r e of this isomerism, it is necessary to consider t h e ways in which isomerism m a y be explained. Upon encountering a new case of isomerism in the laboratory, it is possible to approach its explana­ tion with varying degrees of profundity. Jorgensen, who discovered the flaveo salts and, consequently, t h e isomerism of the flaveo a n d croceo salts, tried to interpret this isomerism from the standpoint of the structures of the co-ordinated nitro groups.

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